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Department of Physical Chemistry of Solids

Head of Department: Professor Stanislaw Filipek
tel. + 48 (22) 343-3334
e-mail: smf@ichf.edu.pl
Pav. 7a, room 224


Research areas:

Gas - solids systems under high pressure of gaseous phase
  • Metal - hydrogen/deuterium systems. Syntheses of novel hydrides/deuterides and their properties.
    • Syntheses of novel metal hydrides/deuterides under high pressure of gaseous hydrogen
    • P(H2/D2) - c(H/D)-T relationships (Pressure - Composition - Temperature diagrams)
    • Amorphous systems
    • Structural studies
    • Transport properties
    • Magnetic properties
    • Diffusion of hydrogen in solids
    • Low-temperature properties of hydrides
    • Equation of State and Phase transitions (including those induced by hydrostatic pressure)
  • Metal-nitrogen and metal oxygen systems under high pressure of gaseous phase

  • Non-equilibrium thermodynamics
  • High pressure technique

Laboratory of High Pressures

Selected papers
  1. B. Baranowski, R. Wisniewski, Bull. Polon. Acad. Sci., 14 (1966) 273.
  2. T. Sko¶kiewicz., Phys. Stat. Sol. (a) 11, K123 (1972).
  3. M. Krukowski, B. Baranowski, J. Less-Common Metals, 49 (1976) 385.
  4. A. Szokefalvi-Nagy, S.M. Filipek and R. Kirchheim,
    "Pressure-Composition Isotherms of Hydrogen in Amorphous Pd-Si"; J.Phys.Chem.Solids Vol. 48 No7 (1987) 613-619.
  5. S.M. Filipek,
    "The Influence of Hydrogen on the Thermoelectric Power of Palladium Based and Nickel Based Alloys", Z. Phys. Chemie NF., 163 (1989) 627.
  6. M. Tkacz,
    "Novel high-pressure technique for loading diamond anvil cell with hydrogen", Polish J. Chem., 69 (1995) 1205.
  7. M. Tkacz,
    "High pressure studies of rhodium-hydrogen system in diamond anvil cell", J. Chem. Phys., 108(5) (1998) 2084.
  8. S.M. Filipek, H. Sugiura, T. Skoskiewicz,
    "Pressure Induced Phase Transformations in the Mn-H and Mn-H/N" AIRAPT-17 Proc. Science and Technology of High Pressure (Murli H. Manghnani, William J. Nellis and Malcolm F. Nicol Eds.) Universities Press, Hyderabad, India 2000 p. 550-554.
  9. A.W. Szafrański,
    "Effect of dissolved hydrogen on electron transport in nickel-chromium alloys", J. Alloys & Comp., 340, 54-61 (2002).
  10. V Paul-Boncour, S M Filipek, G André, F Bourée, M Guillot, R Wierzbicki, I Marchuk, R S Liu, B Villeroy, A Percheron-Guégan, H.D. Yang, S. C. Pin, "Structural, thermal and magnetic properties of ErMn2D6 synthesized under high deuterium pressure", J.Phys.: Condens. Matter 18 (2006), 6409-6420.
  11. S Mylswamy, V Drozd, R S Liu, N C Bagkar, C C Chou, C P Sun, H D Yang, V Paul-Boncour, I Marchuk, S M Filipek, H-S Sheu and L-Y Jang, Structural, electronic and magnetic properties of ErFeMn and ErFeMnH4.7 compounds, New J. Phys., 9 (2007), 271
  12. R. Sato, T. Tsutaoka and S.M. Filipek, "High pressure synthesis and magnetic properties of Dy7Rh3 and Tb7Rh3 hydrides", Journ. Alloys and Comp. 446-447 (2007) 610-613
  13. S.M. Filipek, "Metal Hydrides under High Hydrostatic Pressure", J. Adv. Sci. 18, 1-2 (2007), pp. 1-10
  14. S.M. Filipek, H. Sugiura, V. Paul-Boncour, R. Wierzbicki, R.S. Liu, N. Bagkar; Studies of Novel Deuterides RMn2D6 (R - Rare Earth) compressed in DAC up to 30 GPa, (2008) J. Phys.: Conf. Ser. 121 022001
  15. Ogienko AG, Tkacz M, Manakov AY, Lipkowski J., "First determination of volume changes and enthalpies of the high-pressure decomposition reaction of the structure H methane hydrate to the cubic structure I methane hydrate and fluid methane", J. Phys. Chem. B 111 (44) 12795-12798 2007
  16. Tkacz M, Palasyuk T., "Pressure induced phase transformation of REH3", J. Alloy Comp. 446, 593-597 2007
  17. H. Sugiura, S.M. Filipek, V. Paul-Boncour, I. Marchuk ; Pressure Induced Phase Transitions and EOS Derived for Laves Phase Deuterides ErFe2Dx (x=1.35, 1,9 and 3.4); Polish J. Chem. 82, (2008) 1959-1972
  18. M. Tkacz, T. Palasyuk, J. Graetz, S. Sabena, High-pressure Raman spectroscopy study of a and g polymorphs of ALH3, J. Raman Spectrosc. 39 922-927 (2008)
  19. A.W. Szafrański, "Thermoelectric power of palladium-nickel-hydrogen alloys between 80 and 300 K", Polish. J. Chem. 82, 1949 (2008)
  20. V Paul-Boncour, S M Filipek, R Wierzbicki, G André, F Bourée, M Guillot, Structural and magnetic properties of DyMn2D6 synthesized under high deuterium pressure, J. Phys.: Cond. Mat. 21 (2009) 016001
Review papers
  • B. Baranowski, "Hydrides and Deuterides of Nickel and Copper-Nickel Alloys" in Festkoerperchemie, Beitrage aus Forschung und Praxis (V. Boldyrev and K. Meyer Eds) , VEB Deutscher Verlag fuer Grundstoffindustrie, Leipzig, 1973, 364.
  • B. Baranowski, "Metal Hydrogen Systems at High Hydrogen Pressure", in: Hydrogen in Metals, (G. Alefeld and J. Voelkl Eds), Top. Appl. Phys., vol.29, 1978, 157.
  • B. Baranowski and S.M. Filipek, "Synthesis of Metal Hydrides" in High Pressure Chemical Synthesis, J. Jurczak and B. Baranowski (Eds.), Elsevier, Amsterdam (1989) pp. 55 - 100.
Monographs
  • B. Baranowski, Nichtgleichgewichts-Thermodynamik In der physikalischen Chemie, Leipzig, VEB Deutscher Verlag fuer Grundstoffindustrie, Leipzig, 1975.
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